TY - JOUR
T1 - Sintering behavior and ionic conductivity of Li1.5Al0.5Ti1.5(PO4)3 synthesized with different precursors
AU - Davaasuren, Bambar
AU - Ma, Qianli
AU - Heiden, Alexandra von der
AU - Tietz, Frank
N1 - KAUST Repository Item: Exported on 2021-09-06
Acknowledgements: We thank Dr. D. Grüner (FZJ, IEK-2) for the SEM investigations, M. Andreas and V. Bader for technical assistance, and A. Hilgers for
PSD and M.-T. Gerhards for DTA/TG and dilatometry measurements. We also thank our colleagues at the Central Institute of Engineering, Electronics and Analytics (ZEA-3) for the ICP-OES analysis
PY - 2021/9/3
Y1 - 2021/9/3
N2 - Li1.5Al0.5Ti1.5(PO4)3 (LATP) powders were prepared from different NOx-free precursors using an aqueous-based solution-assisted solid-state reaction (SA-SSR). The sintering behavior, phase formation, microstructure and ionic conductivity of the powders were explored as a function of sintering temperature. The powders showed a relatively narrow temperature windows in which shrinkage occurred. Relative densities of 95% were reached upon heating between 900 and 960 °C. Depending on the morphological features of the primary particles, either homogeneous and intact microstructures with fine grains of about
AB - Li1.5Al0.5Ti1.5(PO4)3 (LATP) powders were prepared from different NOx-free precursors using an aqueous-based solution-assisted solid-state reaction (SA-SSR). The sintering behavior, phase formation, microstructure and ionic conductivity of the powders were explored as a function of sintering temperature. The powders showed a relatively narrow temperature windows in which shrinkage occurred. Relative densities of 95% were reached upon heating between 900 and 960 °C. Depending on the morphological features of the primary particles, either homogeneous and intact microstructures with fine grains of about
UR - http://hdl.handle.net/10754/670932
UR - https://www.degruyter.com/document/doi/10.1515/zpch-2021-3090/html
U2 - 10.1515/zpch-2021-3090
DO - 10.1515/zpch-2021-3090
M3 - Article
SN - 2196-7156
JO - Zeitschrift für Physikalische Chemie
JF - Zeitschrift für Physikalische Chemie
ER -